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Synthesis of Dihydrazine-1,2,4,5-tetrazine Decahydrodecaborate
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(Xi′an Modern Chemistry Research Institute, Xi′an 710065, China)

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    Abstract:

    3, 6-Dihydrazine-1, 2, 4, 5-tetrazine and decahydrodecaboric acid were synthesized from the starting material 3, 6-di(3, 5-dimethyl pyrazole)-1, 2, 4, 5-tetrazine and [N(C2H5)4]2B10H10, respectively. Dihydrazine-1, 2, 4, 5-tetrazine decahydrodecaborate was obtained by neutralization reaction with the yield of 80%. The compound was characterized by IR, 1H NMR, and elemental analysis. Moreover, the combustion heat of the compound determined by oxygen bomb combusion is 37.5 kJ·g-1.

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王为强,薛云娜,梅苏宁,等.双肼基均四嗪十氢十硼酸盐的合成[J].含能材料,2014,22(3):428-429.
WANG Wei-qiang, XUE Yun-na, MEI Su-ning, et al. Synthesis of Dihydrazine-1,2,4,5-tetrazine Decahydrodecaborate[J]. Chinese Journal of Energetic Materials,2014,22(3):428-429.

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History
  • Received:September 20,2013
  • Revised:December 29,2013
  • Adopted:January 16,2014
  • Online: July 01,2014
  • Published: