Crystal Structure of 3,6-Bis(3,5-dimethylpyrazol-1-yl)-1,2,4,5-tetrazine

doi:10.3969/j.issn.1006-9941.2012.06.032

Home > Archive>Volume 20, Issue 6, 2012 >812-813. DOI:10.3969/j.issn.1006-9941.2012.06.032

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School of Mechatronical Engineering of Beijing Institute of Technology,State Key Laboratory of Explosion Science and Technology,Beijing Institute of technology,Beijing,State Key Laboratory of Explosion Science and Technology,Beijing Institute of technology,Beijing,State Key Laboratory of Explosion Science and Technology,Beijing Institute of technology,Beijing,State Key Laboratory of Explosion Science and Technology,Beijing Institute of technology,Beijing,Institute of Chemical Materials,China Academy of Engineering Physics

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Abstract:

3, 6-Bis(3, 5-dimethylpyrazol-1-yl)-1, 2, 4, 5-tetrazine (BT) was prepared by oxidation of 3, 6-bis(3, 5-dimethylpyrazol-1-yl)-1, 2-dihydro-1, 2, 4, 5-tetrazine (BDT) with NO₂. The single crystal was cultured in anhydrous alcohol using slow evaporation method, and was determined by X-ray diffraction analysis. The molecule belongs to monoclinic system, space group P₂(1)/c, with crystal parameters of a=1.096 nm, b=1.651 nm, c=0.714 nm, β=103.895(4) °, Z=4.

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孙谋,张建国,冯金玲,等.3,6-二(3,5-二甲基吡唑-1-基)-1,2,4,5-四嗪的晶体结构[J].含能材料,2012,20(6):812-813.
SUN Mou, ZHANG Jian-guo, FENG Jin-ling, et al. Crystal Structure of 3,6-Bis(3,5-dimethylpyrazol-1-yl)-1,2,4,5-tetrazine[J]. Chinese Journal of Energetic Materials,2012,20(6):812-813.

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Received:June 08,2012
Revised:June 15,2012
Adopted:August 24,2012
Online: December 25,2012
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