A novel energetic material 3, 4-bis-(3′-aminofurazal -4′-yl)-furazan(BATF) was synthesized with yield of 54% using reduction of 3, 4-bis-(3′-aminofurazal-4′-yl)-furoxan (DATF) and DATF was produced by dimerization of 3-aninofurazan-4-carboxchlorid-oxime(AAOF). Its structure was characterized by IR, ¹³C NMR, ¹H NMR, MS and elemental analysis. The split mechanism of BATF was investigated by MS(EI) spectra analysis.The synthetic conditions of reduction were optimized as follows: SnCl₂·2H₂O is reductant in the mixed water solution of HCl and AcOH, n(SnCl₂·2H₂O):n(DATF)is 3:1~4:1, the reaction temperature 75 ℃ and the reaction time 7 h.