Synthesis of 3-Methoxy-5-chloro-2,6-dinitropyridine
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Abstract:
3-Methoxy-5-chloro-2,6-dinitropyridine (the compound Ⅲ) was synthesized from 3,5-dichloropyridine by substitution and nitration. The total yield reached 46%. Its melting point is 115-117 ℃. The structure of the product was identified by IR,1H NMR,MS and element analysis.
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陈军,李全良,王建龙.3-甲氧基-5-氯-2,6-二硝基吡啶的合成[J].含能材料,2007,15(5):500-501. CHEN Jun, LI Quan-liang, WANG Jian-long. Synthesis of 3-Methoxy-5-chloro-2,6-dinitropyridine[J]. Chinese Journal of Energetic Materials,2007,15(5):500-501.