Effect of the First Reaction Time on the Preparation of HMX
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The effects of the first feeding and preservation time on the yield and purity of HMX were studied in the process of synthesis HMX by the way of acetic anhydride. The factors affecting the yield and purity of HMX were discussed. The results show that when the feeding and reserved time are 30 min,the yield and purity of crude HMX and the yield of pure HMX is 67.8%,75.1% and 53.2%,respectively.
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李全良,王建龙,陈军.一段反应时间对HMX制备的影响[J].含能材料,2007,15(2):112-113. LI Quan-liang, WANG Jian-long, CHEN Jun. Effect of the First Reaction Time on the Preparation of HMX[J]. Chinese Journal of Energetic Materials,2007,15(2):112-113.