A new compound 3,5-diamino-2,4-dinitrochlrobenzene was synthesized from sym-trichlorobenzene by nitration and amination. Its melting point is 204~206 ℃. Its structure was proved by FT-IR,NMR,MS and element analysis. And its surface shape was characterized by SEM.
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周红萍,董海山,郝莹,等.3,5-二氨基-2,4-二硝基氯苯的合成研究[J].含能材料,2004,12(2):107-109. ZHOU Hong-ping, DONG Hai-shan, HAO Ying, et al. Synthesis of 3,5-diamino-2,4-dinitrochlrobenzene[J]. Chinese Journal of Energetic Materials,2004,12(2):107-109.