The Synthesis Study of 2,4,7,9,11,14-Hexazatricyclo[8.4.0.03,8]tetradecane
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2,4,7,9,11,14-hexazatricyclo[8.4.0.03,8]tetradecane is synthesized from formamide and 2,3-bishydroxylpiperazine that is the condensation product of ethylenediamine and glyoxal. The total yield of 2,4,7,9,11,14-hexazatricyclo[8.4.0.03,8]tetradecane is 51% by optimizing the reaction conditions (time,temperature,solvent etc.).
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高荣,陆明.2,4,7,9,11,14-六氮杂三环[8.4.0.03,8]十四烷的合成研究[J].含能材料,2002,10(2):53-55. GAO Rong, LU Ming. The Synthesis Study of 2,4,7,9,11,14-Hexazatricyclo[8.4.0.03,8]tetradecane[J]. Chinese Journal of Energetic Materials,2002,10(2):53-55.