CHINESE JOURNAL OF ENERGETIC MATERIALS
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造型颗粒统计特征参量CT量化表征方法
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作者单位:

中国工程物理研究院化工材料研究所, 四川 绵阳 621999

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基金项目:

国家自然科学基金青年基金(12105267)


Quantitative CT Characterization Method for the Characteristic Parameters of Molding Granules
Author:
Affiliation:

Institute of Chemical Materials, CAEP, Mianyang 621999, China

Fund Project:

Grant support: National Natural Science Foundation of China (No. 12105267)

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    摘要:

    为了量化表征造型颗粒结构统计特征参量,基于显微CT、图像处理与统计分析技术开展了造型颗粒统计特征参量表征方法研究,利用该方法对TATB基造型颗粒统计特征参量进行表征并用筛网筛分实验对表征结果进行了验证,对表征结果的稳定性和重复性进行了评估。结果表明,该方法可实现对造型颗粒粒径、形貌、孔隙、密度、堆积特性的量化表征,TATB基造型颗粒的粒径与球形度分别近似服从指数高斯和韦伯分布,本征密度1.35 g·cm-3,可见孔隙率2.3%(空间分辨率14.3 μm),体积分数0.69。评估实验表明该方法具有较好准确性,表征结果具有较好的稳定性和重复性,粒径表征结果与筛网筛分结果相符,主要统计特征参量在不同时间段的测量结果相对偏差小于1%,形貌和孔隙特性表征结果受样品堆积状态影响相对较大。

    Abstract:

    Quantitative characterization of its physical structure is crucial for regulating and enhancing the performance of PBX. Utilizing micro-CT, image processing, and statistical analysis, we researched the quantitative acquisition of characteristic parameters for molding granules. We conducted research on image processing and statistical analysis to quantitatively obtain the characteristic parameters of molding granules based on micro-CT. The characteristic parameters of TATB-based molding granules were characterized by this method, and an evaluation of the characterization method was conducted. The results suggest that this method can implement the quantitative characterization of the size, morphology, porosity, density, and packing characteristics of the molding granules. The granule size and sphericity of the TATB-based molding granules approximately follow the exponential Gaussian and Weibull distributions, respectively. The intrinsic density is 1.35 g·cm-3, with a visible porosity of 2.3%(@spatial resolution 14.3 μm), and a volume fraction of 0.69. Evaluation experiments demonstrate that the method exhibits good accuracy, stability, and repeatability. The characterization results of granule size are consistent with those of the sieving process, and the relative deviation of the characterization results of main characteristic parameters in different periods is less than 1%. The results of morphology and properties are relatively significantly influenced by the packing state of granules and the spatial resolution of micro-CT.

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引用本文

张催,张才鑫,杨亚飞,等.造型颗粒统计特征参量CT量化表征方法[J].含能材料, 2023, 31(12):1262-1268. DOI:10.11943/CJEM2023142.
ZHANG Cui, ZHANG Cai-xin, YANG Ya-fei, et al. Quantitative CT Characterization Method for the Characteristic Parameters of Molding Granules[J]. Chinese Journal of Energetic Materials, 2023, 31(12):1262-1268. DOI:10.11943/CJEM2023142.

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历史
  • 收稿日期: 2023-07-08
  • 最后修改日期: 2023-11-23
  • 录用日期: 2023-11-16
  • 在线发布日期: 2023-11-16
  • 出版日期: 2023-12-25