CHINESE JOURNAL OF ENERGETIC MATERIALS
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水中偏二甲肼及其转化产物检测方法研究进展
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1.北京高科技研究所, 北京 100085;2.西安高科技研究所, 陕西 西安 710025;3.北京农学院国际学院, 北京 102206

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Progress Progess on Detection Methods of UDMH and Its Transformation Products in Water
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1.Hightech Institute of Beijing, Beijing 100085, China;2.Hightech Institute of Xi′an, Xi′an 710025, China;3.College of International Education, Beijing University of Agriculture, Beijing 102206, China

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    摘要:

    水中偏二甲肼(UDMH)及其转化产物的快速检测对于其污染控制具有重要意义。本文梳理了色谱法(包括气相色谱、高效液相色谱和离子色谱)和非色谱法(包括电化学法、分光光度法、化学发光法)对水中UDMH的检测研究进展,并简要介绍了色谱法在水中UDMH转化产物检测方面的应用研究,指出了不同检测方法在检测浓度范围、样品前处理、抗干扰能力等方面的优缺点,认为色谱前处理装置的高效自动化设计、多种分离和检测技术联用是解决水中UDMH和其转化产物检测难题的未来发展方向。

    Abstract:

    Rapid detection of unsymmetrical dimethylhydrazine (UDMH) and its transformation products in water is of great significance for its pollution control. This paper reviewsthe research progress of chromatographic methods (including gas chromatography, high performance liquid chromatography, and ion chromatography) and non-chromatographic methods (including the electrochemical method, spectrophotometry and chemiluminescence) in the detection of UDMH in water. Then, application of chromatography in in the detection of UDMH conversion products in water was briefly introduced. The advantages and disadvantages of different detection methods in the detection concentration range, sample pretreatment and anti-interference ability, etc.,were pointed out. It was suggested that the design of efficient automatic chromatographic pretreatment device and the combination of various separation and detection technologies would be the future development direction to solve the detection problem of UDMH and its transformation products in water.

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高鑫,杨玉雪,卢忻,等.水中偏二甲肼及其转化产物检测方法研究进展[J].含能材料, 2022, 30(6):611-621. DOI:10.11943/CJEM2021154.
GAO Xin, YANG Yu-xue, LU Xin, et al. Progress Progess on Detection Methods of UDMH and Its Transformation Products in Water[J]. Chinese Journal of Energetic Materials, 2022, 30(6):611-621. DOI:10.11943/CJEM2021154.

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历史
  • 收稿日期: 2021-06-16
  • 最后修改日期: 2022-04-24
  • 录用日期: 2021-12-08
  • 在线发布日期: 2022-01-13
  • 出版日期: 2022-06-25