Six kinds of substituted piperazine were synthesized,and the structures of these compounds were identified by 1HNMR、IR and elemental analysis. 4,10-dinitro-2,6,8,10-tetraoxa-4,10-diaza-tetrecyclo[5.5.0.05,903,11]-dodecane(TEX) was synthesized by nitrating these matrixs in different yields respectively, and the stability of the substituted piperazine explained why the yields were different.
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李战雄,欧育湘,陈博仁.由不同取代哌嗪合成TEX[J].含能材料, 2001, 9(3):104-106. LI Zhan-xiong, OU Yu-xiang, CHEN Bo-ren. Synthesis of TEX from Six Kinds of Different Substituted Piperazine[J]. Chinese Journal of Energetic Materials, 2001, 9(3):104-106.