CHINESE JOURNAL OF ENERGETIC MATERIALS
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基于分形维数的老化NEPE推进剂拉伸损伤演化表征与分析
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1.内蒙古工业大学理学院;2.青海大学土木水利学院;3.中国航天科工集团第六研究院四十一所;4.中国航天科工集团第六研究院四十六所

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Characterization and Analysis of Tensile Damage Evolution in Aged NEPE Propellant Based on Fractal Dimension
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1.College of Science,Inner Mongolia University of Technology;2.College of Civil and Hydraulic Engineering, Qinghai University;3.The st Research Institute of the Sixth Research Academy, China Aerospace Science and Industry Corporation

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    摘要:

    为定量研究老化前后硝酸酯增塑聚醚(Nitrate Ester Plasticized Polyether,NEPE)推进剂在拉伸下的表面细观损伤,开展了不同老化时间(0,7 d,40 d,80 d)的热加速老化实验,采用场发射电子显微镜(FE-SEM)配合原位拉伸台进行了原位拉伸实验并数字化处理了拍摄图像。采用分形维数定量化表征分析了推进剂不同老化阶段细观损伤演化过程,研究了老化前后推进剂孔隙率法与分形维数法在细观损伤表征上的差异。结果表明:分形维数能有效表征不同老化阶段NEPE推进剂的表观损伤过程。当伸长率小于20%时,分形维数随伸长率增加而增大,且增速较快;当伸长率在20%~60%时,分形维数仍随伸长率增加而增大,但增速放缓,并发现老化时间越长,分形维数与伸长率的线性关系更显著的规律;当伸长率大于60%后,不同老化阶段推进剂分形维数随伸长率呈不规则变化。孔隙率法与分形维数法对比表征老化前后推进剂拉伸过程存在差异,且老化后差异更加显著,孔隙率法主要量化孔隙面积占比,分形维数法则表征表面形貌的粗糙度与复杂度特征。

    Abstract:

    To quantitatively investigate the evolution of surface mesoscopic damagein nitrate ester plasticized polyether (NEPE) propellant during tension before and after aging, thermal accelerated aging tests were conducted with different aging days (0, 7 d, 40 d, 80 d). An in-situ tensile machine combined with field emission scanning electron microscopy (FE-SEM) was employed for in-situ tensile testing, after which the captured images underwent digital processing. The fractal dimension was applied to quantitatively characterize and analyze the evolution of mesoscopic damage in the propellant at different aging stages. The differences between porosity method and fractal dimension method in characterizing mesoscopic damage before and after aging were studied. Results indicate that fractal dimension successfully captures the apparent damage evolution of NEPE propellant over different aging stages. During tension, for elongation below 20%, the fractal dimension rises relatively quickly with elongation. In the 20%-60% elongation range, the fractal dimension still increase with elongation, though at a reduced rate. Moreover, longer aging times were found to enhance the linear correlation between fractal dimension and elongation in this stage. Beyond 60% elongation, the fractal dimension shows irregular variation with elongation for all aging stages. Differences emerged between the porosity method and the fractal dimension method when characterizing the tensile process, especially after aging. While the porosity method mainly measuresthe area fraction of pores, the fractal dimension method characterizes the roughness and complexity of the surface morphology.

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引用本文

张涛,姬永超,李卓,等.基于分形维数的老化NEPE推进剂拉伸损伤演化表征与分析[J].含能材料, 2026, 34(2):130-137. DOI:10.11943/CJEM2025163.
ZHANG Tao, JI Yong-chao, LI Zhuo, et al. Characterization and Analysis of Tensile Damage Evolution in Aged NEPE Propellant Based on Fractal Dimension[J]. Chinese Journal of Energetic Materials, 2026, 34(2):130-137. DOI:10.11943/CJEM2025163.

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  • 收稿日期: 2025-07-11
  • 最后修改日期: 2025-12-30
  • 录用日期: 2025-12-15
  • 在线发布日期: 2025-12-22
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